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AGITATED NUTSCHE FILTER DRYER

Agitated nutsche filter dryer

RAVI – Agitated nutsche filter dryer is versatile units designed for multipurpose production facilities. To meet the demanding requirements for filters used in the manufacture of pharmaceutical ingredients, the filters are designed to meet stringent cGMP and FDA guidelines. To allow for good cleanability using CIP systems and to permit optimal inspection after the cleaning process all product wetted surfaces are designed without dead areas, with smooth transitions of internals and without any bolted connections. For good access to the filter internals for cleaning and inspection purposes the filters are equipped with an openable filter base. 

The overall attention to design details allows for simplified validation of the units. The agitator is supported from the top, with the agitator drive, the bearings and the shaft seal installed externally. Shaft sealing is with a double mechanical seal and a convoluted bellows. The agitator arms with specially designed bottom smooth surface and press the cake when rotated counter clockwise, and mix and agitate the cake when rotated clockwise.

Simultaneous rotational and vertical agitator motions result in a very efficient and even mixing of the entire product mass for mixing and drying.  The agitator arms are S-shaped for improved product discharge.

All product wetted surfaces are heated to obtain the largest possible heat exchange area for short drying times and a low attainable final  humidity.

CONSTRUCTION :

Additionally, the equipment is fitted with a stirrer mechanism which efficiently agitates the slurry during cake washing, smoothes and squeezes the cake during filtration and assists in the automatic discharge of the cake. A side discharge arrangement is provided, closing and opening through hydraulic / mechanical means. A filter plate with filter cloth is fitted at the bottom of the shell for separating liquids from solids. The cake is retained on top of the plate. The upward and downward movement of the agitator assembly is utilized for cake washing, compressing, drying and discharge of the cake. A vacuum pump connected to receiver is installed for discharging of liquids and vapor collection. The cylindrical shell can also be provided with a jacket. A filter plate is located at the base of the vessel in level with the discharge port. The filter medium, usually a filter cloth, is fitted on the filter plate which is replaceable type.

In addition a special multilayered filter plate can also be provided instead of filter cloth. In dryer construction heating is provided on shell by limpet in bottom by jacket and through hollow agitator and blades. Vacuum is applied for fast drying.

It has multi- functional utility, saves on power, labor, floor space, material wastage and time. We use sophisticated technology that combines hydraulics and agitation, which makes the Agitated filter dryer easy to use and very versatile.

 

SALIENT FEATURES :

  • Designed and Manufactured to suit critical hygienic conditions of pharma and food industries. (cGMP MODEL).
  • Operated by hydraulic cylinders and held tightly with zero leakage.
  • Offered in various materials of constructions, like stainless steel, Hastelloy, Titanium, carbon steel, rubber lined carbon steel and lead lined carbon steel.
  • Offered in a wide range of filtration area capacities from 25 Lits upto 10000 Lits.
  • Method of operation is totally enclosed, neat and hygienic. These conditions are excellent for solvent recovery, Hollow Shaft and Hollow Blades for thorough drying.
  • Suitable for handling of sterile compounds or toxic and hazardous materials without human intervention.
  • Enables easy non-manual and automatic cake / solid discharge. Scraper blade is provided to scrap the material which may stay on shell.
  • Hollow Shaft and Hollow Blades for thorough drying.
  • Specially designed tank cleaning nozzle is provided for thorough cleaning of inside of filter body. (CIP)
ANFD in Pharma
Agitated nutsche filter dryer working principle

TECHNICAL DESIGN PARAMETERS :

 Design Pressure Vessel -Full Vaccum , Jacket/Limpet – 4bar
 Design Temp 150deg
 Finish Internal: 240gr Mirror finish, External 180gr Mat finish
 
OPERATIONAL SEQUENCE :
The operation of Nutsche Filters requires a complex manipulation of valves and hydraulics so present day installations are always semi or fully automated.
 
Filtration
The filter is charged with slurry and pressure is applied to displace the filtrate leaving the cake retained over the filter medium. For slurries with a wide distribution of coarse fast settling solids and slow settling fines there is a risk of segregation with the finer fraction settling over the coarse fraction. When this happens the fines seal the cake and slow down the cake formation so keeping the slurry in suspension with rotating arms during filtration assists in forming a homogeneous cake.
 
Cake Washing

In the washing stage a spray ring or connections on top of the cover introduce the wash liquid over the cake. This displaces the mother solution with the wash liquid but with such in-situ washing the efficiency may be quite low if the cake forms with an uneven thickness.

One of the advantages of the Nutsche Filter is the ability to smoothen the cake’s surface prior to applying spray wash so that the entire bed is washed evenly.

Washing efficiency may be further improved if air or gas are not allowed to enter the cake in a multi-washing system so the wash liquids always displace the solutions in a “piston” like manner. This is achieved by a special detector that monitors the surface of the cake for moisture and once air or gas start entering the bed a signal is transmitted to close the filtrate valve and reopen it once next washing commences.

 
Cake Repulping
Many processes require high washing efficiency to remove the contaminating liquid from the product and washing the cake by repulping yields the most efficient product purity. This is done by resuspending the cake with the paddle arms for thorough mixing with the wash solution. During resuspension the rotating arms are moving slowly downwards and are “shaving” the bed gradually layer after layer until the entire cake enters the slurry.
 
Pressure Drying

In the drying stage air or gas purges the cake until the captive moisture is reduced to an asymptotic level and in practical terms the cake is considered to be as dry as possible.

To obtain minimum moisture the cake is smoothened by reversing the rotation of the paddle or auger arms and exerting controlled pressure on its surface with the hydraulic system. This seals cracks in the cake so that air or gas will not bypass the bed.

 
Vacuum Drying
Further reduction in cake moisture may be obtained by slowly rotating and lowering the paddle arms to scrape and de-lump the cake. To take advantage of the drying ability of the Nutsche Filter it is worth considering the option of heating components such as the vessel, filter floor and paddles to enhance drying.
 
Cake Discharge

Once all the stages are completed the cake discharge valve opens and the paddle arms on the smaller machines or the auger arms on the larger ones are rotated and lowered to convey the dry cake towards the center. The same procedure also applies to side discharge machines however it should be noted that in this case the cake comes out intermittently and not continuously. This may have a layout impact on the downstream facility such as the conveyor that handles the product to storage.

On some filters the cloth or woven mesh screen may be backwashed with water to dislodge and remove any cake residue that adhered to the medium after cake discharge.

TECHNICAL SPECIFICATIONS :

MODEL

CAPACITY IN LTRS.

FILTER
AREA M2

CAKE VOLUMN LTR

DIMENSION DIA  mm”D”

DIMENSION TOTAL HT
mm “HT”

VERTICAL STROKE
mm “S”

DRIVE MOTOR  HP

RV-ANFD
500

500

0.56

200

900

3300

200

2.0

RV-ANFD 1000

1000

1

400

1200

3350

350

3.0

RV-ANFD 1500

1500

1.5

600

1500

3500

400

5.0

RV-ANFD 2000

2000

2

800

1600

3500

400

7.5

RV-ANFD 3000

3000

2.83

1200

2000

3700

400

7.5

RV-ANFD 4000

4000

3.33

1600

2200

3900

450

12.5

RV-ANFD 5000

5000

4.81

2000

2600

3900

500

15.0

RV-ANFD 7000

7000

6.43

2800

3000

4200

600

20.0

RV-ANFD 10000

10000

8.81

4000

3500

4350

600

25.0

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